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Continuing S e r i e s A Volume 63 November A carrying out precipitations from homogeneous solutions. One of the most serious deficiencies of this book, in this reviewer's opinion, is the lack of emphasis on the tremendous importance of the sampling step in the analytical process.
Chapter 1covers the analytical process, but fails to warn the reader that unless the sample is properly obtained, the rest of the process is largely a waste of time and effort. Chapter 2 mentions that the sampling process "can be the most critical aspect of an analysis", but this statement is both too weak and too late.
In clinical chemistry, for example, far too many diagnoses are made incorrectly because a phlehotomist was careless in mixing the sample, or a non-fasting sample was obtained.
Many features of this edition are very worthwhile. For example, the description of the electronic balance, the treatment of error propagation including logarithm and significant figures , and the use of Gibbs free energy in treating equilibria are all done well. Likewise, the introduction of ion chromatography and flaw injection analysis and the use of internal standards and standard additions in atomic absorption spectrophotometry is very helpful. The chapter on clinical chemistry is most deficient.
The first two tables ambiguously distinguish between serum and "blood" samples, where t h e author sometimes means whole blood and sometimes means plasma. It is unfortunate that much of the data in Table The experiments include a wide variety of representative techniques and are now collected together a t the end of the text grouped by topic.
There should he no trouble selecting worthwhile experiments that capture the student's interest. Although this book has some minor deficiencies, the scope and clarity of mast aspects of "Analytical Chemistry" is commendable, and the text merits serious consideration for adoption. This book covers all the current largescale crystal growth methods, with a systematic treatment of the technological and economic factors involved.
The author begins with an overview of the major uses of crystals, the classification of growth processes, and hasic conceptual theory. Each production process is then described in detail, covering both theory and practice. The text draws attention to the similarities between processes ta emphasize that only a few principles are involved. New York, NY, New York, NY. McHughand Val J. Butterworlh Publishers, Boston, MA.
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